热处理改善热压烧结成型GH4099高温合金微观组织和力学性能

Heat treatment improves the microstructure and mechanical properties of hot isostatic pressing formed GH4099 superalloy

  • 摘要: 本文采用固溶后时效处理的工艺研究了热处理制度对热压烧结成型GH4099高温合金微观组织演变及其对力学性能优化的影响。结果表明,采用1200℃和130MPa的热压烧结工艺保温4h,可以成功制备致密度优良的GH4099高温合金。合金的微观组织主要由等轴晶粒组成,平均晶粒尺寸为38μm,晶界处连续分布了大量的碳化物,且在该工艺下仍保留了部分清晰的原始颗粒的边界。成型后的合金屈服强度为700MPa,抗拉强度为1167MPa,延伸率为27.91%。固溶处理并未显著影响热压烧结后合金的晶粒尺寸,但改善了晶粒内和晶界碳化物的分布,这使得合金强度和延伸率均得到了改善。在1100℃固溶2h随后在800℃时效8h处理的试样屈服强度增加到789MPa,抗拉强度增加到1207MPa,延伸率增加到29.23%。

     

    Abstract:   This paper investigates the influence of heat treatment systems on the microstructure evolution and mechanical property optimization of hot-pressed sintered GH4099 superalloy by using solution treatment followed by aging processes. The results show that the GH4099 superalloy with excellent density can be successfully prepared by using the hot isostatic pressing process at 1200℃ and 130MPa for 4 hours. The microstructure of the alloy is mainly composed of equiaxed grains with an average grain size of 38 μm. A large amount of carbides are continuously distributed at the grain boundaries, and the boundaries of some original particles are still clearly retained under this process. The yield strength of the formed alloy is 700.42 MPa, the tensile strength is 1167.21 MPa, and the elongation is 27.91%. Solution treatment had no significant effect on the grain size of hot-press sintered GH4099 superalloy, but improved the distribution of intragranular and grain boundary carbides, thereby enhancing both the strength and elongation of the alloy. The sample treated with solution treatment at 1100°C for 2 hours followed by aging at 800°C for 8 hours had a yield strength increased to 789.53 MPa, a tensile strength increased to 1207.23 MPa, and an elongation increased to 29.23%.
      Keyworlds: Hot pressed sintering, powder metallurgy, GH4099 superalloy, microstructure, mechanical properties

     

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