强磁场下Nb3Sn超导纤维材料相稳定性预测研究强磁场下Nb3Sn超导纤维材料相稳定性预测研究

Prediction of phase stability of Nb3Sn superconducting fiber materials under high magnetic field

  • 摘要: 为提升材料在高场磁体中的性能,理解材料在复杂环境下的行为,研究强磁场下Nb3Sn超导纤维材料相稳定性预测,球磨混合铌粉,锡粉,铁粉这三种粉末原料,经过压制、烧结、抛光等多道工艺处理之后得到Nb3Sn超导纤维材料,将该材料置于强磁场热处理装置中处理后,通过试验预测不同处理方式、不同磁场强度、退火温度以及球磨时间下,该材料的相稳定性。预测结果显示,使用强磁场热处理能明显提升材料相稳定性,球磨时间设定为2.8h,原料晶粒适中,各磁参数较高;7.5T磁场强度下材料富Nb相发生明显取向作用,晶粒光滑度提升。退火温度650℃下,材料富Nb相明显,且分布均匀性较强,晶粒间以层状形态出现大量富Nb相,材料相稳定性较高。

     

    Abstract: In order to improve the performance of materials in high-field magnets, understand the behavior of materials in complex environments, and study the phase stability prediction of Nb3Sn superconducting fiber materials under strong magnetic fields, Nb3Sn superconducting fiber materials were obtained by ball milling mixed with niobium powder, tin powder, and iron powder after multi-process processing such as pressing, sintering, and polishing. After the material was treated in a high magnetic field heat treatment device, the phase stability of the material was predicted by experiments under different treatment methods, different magnetic field intensity, annealing temperature and milling time. The results show that the phase stability of the material can be significantly improved by using high magnetic field heat treatment. The milling time is set to 2.8h, the grain size of the raw material is moderate, and the magnetic parameters are high. At 7.5T magnetic field intensity, the NB-rich phase of the material has obvious orientation, and the grain smoothness increases. At the annealing temperature of 650℃, the NB-rich phase is obvious, and the distribution uniformity is strong, and a large number of NB-rich phases appear in the layered morphology between the grains, and the phase stability of the material is high.

     

/

返回文章
返回