轧制变形量对2507双相不锈钢组织和性能的影响

Effect of rolling deformation amount on microstructure and properties of 2507 Duplex Stainless Steel

  • 摘要: 通过不同变形量的冷轧工艺和1273K下1分钟退火处理工艺制备具有异质结构特征的 SAF2507 双相不锈钢样品,采用扫描电镜(SEM)、电子背散射衍射(EBSD)、透射电子显微镜(TEM)和电化学测试等技术研究分析了SAF2507合金的物相组成、显微组织分布和耐腐蚀性能,利用准静态拉伸和循环加载试验分析不同结构状态的显微组织对合金力学性能的影响,并分析了其强韧化机制。结果表明:随着轧制变形量的增加,异构样品中铁素体和奥氏体相的晶粒尺寸得到明显细化,两相晶粒的几何必须位错密度显著增加。与粗晶样品相比,轧制退火样品在晶界、相界和孪晶界两侧表现出异质区边界影响区域,存在明显的应变梯度,使得其在拉伸变形过程中产生异质变形诱导(HDI)强化和应变硬化。其中90%-1273样品综合性能最优,表现出更好的耐腐蚀性,屈服强度为715MPa,抗拉强度为939 MPa,均匀延伸率为24.8%,在显著提升强度的同时保持了良好延展性,克服了金属材料强度与延展性的倒置关系(trade-off)。

     

    Abstract: SAF2507 duplex stainless steel samples featuring heterostructured characteristics were fabricated via cold rolling at various reduction rates followed by annealing at 1273K for 1minute. The phase composition, microstructure distribution, and corrosion resistance of SAF2507 alloy were investigated and analyzed using scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), transmission electron microscopy (TEM),and electrochemical testing.Furthermore, the influence of diverse microstructural states on mechanical properties was evaluated through quasi-static tensile and cyclic loading tests to elucidate the underlying strengthening and toughening mechanisms. The results indicate that increasing the rolling reduction significantly,the grain sizes of ferrite and austenite phases in the heterogeneous samples are significantly refined, and the geometrically necessary dislocationsdensity of the two-phase grains increases significantly.Compared with the coarse-grained sample, the rolled and annealed sample exhibits heterogeneous zone boundary affected regions on both sides of grain boundaries, phase boundaries, and twin boundaries, showing a distinct strain gradient. This leads to heterogeneous deformation-induced (HDI) strengthening and strain hardening during tensile deformation.Consequently, the 90%-1273 specimen exhibited the optimal synergy of mechanical properties,demonstrating better corrosion resistance, with a yield strength of 715MPa, a tensile strength of 939MPa, and a uniform elongation of 24.8%. This microstructural design significantly enhanced strength while maintaining excellent ductility, thereby effectively overcoming the strength-ductility trade-off dilemma typically observed in metallic materials.

     

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