大层厚SLM制备GH3536合金组织性能研究

Study on the forming efficiency, microstructure and properties of GH3536 alloy prepared by SLM with large layer thickness

  • 摘要: 为应对GH3536合金SLM常用小层厚(20-40μm)带来的层数多与效率受限问题,本文在80μm铺粉层厚条件下设计并验证了GH3536合金的高效成形参数窗口。设置线间距0.11/0.12mm、激光功率400/430/450W、扫描速度950-1250mm∙s-1,形成T1–T16共16组参数,并采用固溶处理和热等静压+固溶两种热处理方式。采用SEM、EDS、XRD、显微维氏硬度与室温拉伸开展微观组织和力学性能评估。结果表明,固溶处理后熔池边界消失并出现再结晶相关组织特征,孔洞较打印态减少。当扫描速度提高,组织晶粒逐渐细化,出现“大晶粒表面伴生小晶粒”的非均匀特征,析出相由颗粒状转变为线条状,断后延伸率稳定在50%,屈服强度、抗拉强度和维氏硬度略有提高。当激光功率升高,组织晶粒逐渐粗化,析出相变化较小,断后延伸率稳定在50%左右;屈服强度、抗拉强度和维氏硬度略有下降。试样断裂机制主要为在沿晶断裂中存在韧窝的复杂断裂机制。本研究条件下最佳打印工艺为:层厚80μm、线间距0.12mm、激光功率430 W、扫描速度1150mm∙s-1

     

    Abstract:  To address the high number of layers and limited efficiency associated with the commonly used small layer thickness (20-40 μm) in Selective Laser Melting (SLM) of GH3536 alloy, this study designed and validated an efficient processing parameter window for GH3536 alloy using an 80 μm powder layer thickness. A total of 16 parameter sets (T1–T16) were established by varying the hatch spacing (0.11/0.12 mm), laser power (400/430/450 W), and scanning speed (950-1250 mm∙s⁻¹). Two post-heat treatment conditions, namely solution treatment and hot isostatic pressing plus solution treatment, were applied. The phase constitution, microstructure, and mechanical properties were evaluated using SEM, EDS, XRD, micro-Vickers hardness testing, and room-temperature tensile testing. The results indicate that after solution treatment, melt pool boundaries disappear, and recrystallization-related microstructural features emerge, with porosity reduced compared to the as-built condition. As the scanning speed increases, the grain structure gradually refines, exhibiting a heterogeneous "small grains associated with large grain surfaces" characteristic; precipitates transition from a granular to a linear morphology. The elongation after fracture remains stable around 50%, while yield strength, ultimate tensile strength, and microhardness show a slight increase. With increasing laser power, the grains gradually coarsen, precipitates show minimal change, and elongation after fracture remains stable at approximately 50%; however, yield strength, ultimate tensile strength, and microhardness exhibit a slight decrease. The fracture mechanism of the specimens is primarily a complex mixed mode involving intergranular fracture with dimples present. Within the conditions of this study, the optimal printing parameters identified are: layer thickness of 80 μm, hatch spacing of 0.12 mm, laser power of 430 W, and scanning speed of 1150 mm∙s⁻¹

     

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