GH4706合金长时时效下组织转变及拉伸-持久性能规律研究

Research on Microstructure Transformation and Tensile- Rupture Properties of GH4706 Alloy under Long-Term Aging

  • 摘要: 为揭示长时时效对其拉伸-持久性能及微观组织的影响,基于GH4706合金在600、650和675 ℃的时效温度与3000h、5000 h的时效时间条件下,分析了经室温拉伸和持久后的微观组织、断口形貌和力学性能。结果表明:(1)晶粒尺寸随时效温度/时间的增加显著增大,高温长时时效易发生混晶现象;(2)碳化物与η相析出呈现“低温离散-中温致密-高温粗化”规律,η相由离散颗粒状转变为连续针状;(3)断裂模式由韧性断裂向沿晶脆性断裂转变,但持久载荷下析出弥散状碳化物可延缓转变过程;(4)综合拉伸与持久测试结果确定工艺窗口,时效温度需控制不高于650℃,时效时间为3000h,实现组织-性能的调控。

     

    Abstract: To reveal the influence of long-term aging on the tensile- rupture properties and microstructure of GH4706 alloy, the microstructure, fracture morphology and mechanical properties after tensile at room temperature and rupture tests were analyzed for aging temperatures of 600, 650 and 675 ℃ and aging times of 3000 h and 5000 h. The results show that: (1) The grain size increases significantly with the increase of aging temperature/time, and mixed crystal phenomenon is prone to occur at high temperature and long aging time; (2) The precipitation of carbides and η phase follows the rule of "discrete at low temperature - dense at medium temperature - coarsening at high temperature", and the η phase changes from discrete particles to continuous needles; (3) The fracture mode changes from ductile fracture to brittle fracture, but the precipitation of dispersed carbides under enduring load can delay the transformation process; (4) Based on the comprehensive results of tensile and rupture tests, the process window is determined, with the aging temperature controlled not higher than 650 ℃ and the aging time of 3000 h, to achieve the control of microstructure- properties.

     

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