固溶冷却介质对一种难变形镍基高温合金显微组织和力学性能的影响

Effect of cooling method after solution treatment on heat-treated microstructure and mechanical properties of a novel hard-deform nickel-base superalloy

  • 摘要: 本文研究了固溶冷却介质(水冷、油冷、空冷)对一种高γʹ相含量(~55wt.%)镍基变形高温合金热处理组织及力学性能的影响。亚固溶(低于γʹ相全溶温度)静态再结晶晶粒均匀细小(10μm ~30μm)。固溶冷却介质对静态再结晶晶界和γʹ相分布和尺寸产生重要的影响,随着固溶冷速降低(水冷>油冷>空冷),一次γʹ相和二次γʹ相尺寸增加,三次γʹ相数量降低。室温和850℃拉伸强度与二次γʹ相分布紧密相关,二次γʹ相尺寸越小,拉伸强度越高。再结晶晶界状态(和晶粒尺寸)在很大程度上决定了850℃拉伸塑性和850℃/350MPa持久性能。再结晶晶界上一次γʹ相和碳化物的存在有助于850℃断裂形貌具有准解理和塑性混合断裂特征。

     

    Abstract: It is investigated that the effect of solid-solution cooling methods on the heat-treated microstructure and resultant mechanical properties of a novel Ni-based wrought superalloy with a high content of (~55 wt.%) of γʹ phase. The obtained microstructure after sub-solvus static recrystallization is uniform and fine with 10~30 μm. The solid-solution cooling method has a significant impact on the recrystallized grain boundary and the distribution and size of γʹ precipitates. As the solid-solution cooling rate decreases (water cooling > oil cooling > air cooling), the sizes of primary and secondary γʹ precipitates increase, while the number of tertiary γʹ precipitates decreases. The tensile strengths at room temperature and 850 ℃ are closely related to the distribution of γʹ precipitates, and the smaller the size of secondary γʹ precipitates, the higher the tensile strength. Both the tensile plasticity at 850 ℃ and the stress-rupture property under 850 ℃/350 MPa are largely determined by the recrystallized grain boundary (and the grain size). The quasi-cleavage and plastic mixed fracture can be obtained with the presence of coarsened primary γʹ precipitates and carbides on recrystallized grain boundaries at 850 ℃.

     

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