GH4706合金在不同时效下的析出相演化及其对力学性能的影响

Precipitate Phase Evolution of GH4706Alloys under Different Aging Conditions and Its Impact on Mechanical Properties

  • 摘要: 本研究系统探讨了不同时效温度(600℃与650℃)及时效时间(3000h、5000h、10000h)对GH4706合金微观组织演变及其室温拉伸与高温持久性能的影响。结果表明:随时效温度升高与时间延长,晶粒尺寸显著增大,其中650℃-10000h时效后晶粒尺寸达125μm;高温长时时效后,晶界η相由弥散颗粒加速演变为连续网状,同时晶内碳化物(主要为MC和M23C6型)持续粗化,在650℃-10000h条件下最为严重;经室温拉伸后的样品,其断后伸长率对时效温度更敏感,而抗拉强度对时效时间更敏感;经高温持久后的样品,其性能则严重受制于析出物类型,M23C6型碳化物与η相共同作用促进裂纹萌生与扩展,导致650℃-10000h试样持久寿命急剧下降。综上,GH4706合金在高温长期服役中的性能退化核心机制是晶界η相连续网格化与碳化物粗化共同引发的晶界脆化,影响其力学性能。

     

    Abstract: Abstract: This study systematically investigates the effects of different aging temperatures (600℃ and 650℃) and aging times (3000h、5000h、10000h) on the microstructural evolution, room-temperature tensile properties, and high-temperature stress rupture properties of GH4706 alloy. The results indicate that the microstructure coarsens significantly with increasing aging temperature and time, with the grain size reaching 125 μm after aging at 650℃-10000h. Following high-temperature aging, the grain boundary η phase evolves rapidly from dispersed particles into a continuous network, while the intragranular carbides (primarily MC and M23C6 types) undergo continuous coarsening. This process is most severe under the 650℃-10000h condition. The study reveals that during room-temperature tensile testing, the elongation after fracture is more sensitive to temperature, whereas the ultimate tensile strength is more sensitive to time. The high-temperature stress rupture performance is critically dependent on the grain boundary condition; M23C6 carbides and the η phase act synergistically to promote crack initiation and propagation, leading to a drastic reduction in the stress rupture life of the 650℃-10000h sample. In conclusion, the core mechanism behind the performance degradation of GH4706 alloy during high-temperature long-term service is grain boundary embrittlement, induced by the combined effects of the continuous network of grain boundary η phase and the coarsening of carbides, which collectively deteriorate its mechanical properties.

     

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